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KMID : 1059519850290050539
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Journal of the Korean Chemical Society
1985 Volume.29 No. 5 p.539 ~ p.542
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A New Route to Diethyl 3,4,5-Trimethoxybenzylmalonate, a Trimethoprim Intermediate
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Chung Bong-Young
Lee Chae-Ho
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Abstract
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Direct condensation of 3,4,5-trimethoxybenzoyl chloride with diethyl malonate followed by chlorination and hydrogenolysis afforded diethyl 3,4,5-trimethoxybenzylmalonate in 70% overall yield.
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